A new approach to the determination of silicon in zinc, lead-bearing materials and in waste using the ICP-OES method
Authors:
- Artur Przybyła,
- Joanna Kuc,
- Zbigniew Wzorek
Abstract
This work describes the implementation of the ICP-OES silicon determination method for zinc and lead-bearing materials and waste at the Mining and Metallurgical Works ZGH "Bolesław". The proposed method was validated. On the basis of linearity tests, it was found that the course of the calibration curve is linear up to a silicon concentration of 100 mg/L, with the determined working range being 0.10–50%. Precision tests, on the basis of which the repeatability was checked, were carried out for nine types of real samples: zinc sulfides, zinc oxides, zinc-lead ore, lead sulfide and zinc-bearing waste. Real samples and six certified reference materials were tested using the ICP-OES radial position. The identified interferences of molybdenum, chromium and vanadium did not statistically significantly affect the measurement results.
- Record ID
- CUTd2350e29fdb44a289cea8753cce3b871
- Publication categories
- ;
- Author
- Journal series
- Molecules, ISSN , e-ISSN 1420-3049, Biweekly
- Issue year
- 2022
- Vol
- 27
- No
- 10
- Pages
- [1-14]
- Article number
- 3059
- Other elements of collation
- tab.; wykr.; Bibliografia (na s.) - 12-14; Bibliografia (liczba pozycji) - 35; Oznaczenie streszczenia - Abstr.; Numeracja w czasopiśmie - Vol. 27, Iss. 10
- Substantive notes
- Section: Inorganic Chemistry
- Keywords in English
- silicon, ICP-OES, zinc and lead concentrates, waste
- ASJC Classification
- DOI
- DOI:10.3390/molecules27103059 Opening in a new tab
- URL
- https://www.mdpi.com/1420-3049/27/10/3059 Opening in a new tab
- Language
- eng (en) English
- License
- Score (nominal)
- 140
- Score source
- journalList
- Score
- Publication indicators
- Additional fields
- Indeksowana w: Web of Science, Scopus
- Uniform Resource Identifier
- https://cris.pk.edu.pl/info/article/CUTd2350e29fdb44a289cea8753cce3b871/
- URN
urn:pkr-prod:CUTd2350e29fdb44a289cea8753cce3b871
* presented citation count is obtained through Internet information analysis, and it is close to the number calculated by the Publish or PerishOpening in a new tab system.